Institut Charles Sadron (ICS), 23 rue du Loess, BP 84047, 67034 Strasbourg Cédex 2, France
Équipe "Théorie et Simulation des Polymères" (ETSP)
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Current research focus

Glass transition in thin polymer films

Thin polymer films are relevant for many technical applications and phenomena, such as packaging, barriers, membranes, medicine (implants, senors, drug release), tribology, or thin ion conducting polymers. The dynamical properties of polymers confined in thin films can differ significantly from that of bulk properties. For instance, the glass transition point can be altered drastically with respect to its bulk value, and hence, thin polymer films provide an excellent sample geometry for studying finite-size effects on glass forming materials.

The simulation group at the ICS as recently demonstrated these effects.[1] We do molecular dynamics simulations for supported (see panel on the left) and free-standing thin films of non-entangled polymers using a coarse grained (bead-spring) polymer model. The free-standing films (not shown) can be obtained in periodic simulation boxes (without walls). Our research is mainly concerned with the equilibrium properties of the films above the critical temperature Tc(h) of the mode coupling theory. We also determine the glass transition temperature Tg(h) by measurements of the film thickness h upon cooling.

We explore the influence of confinement on the structure and dynamics of the polymer films. We find that the dynamics in the films is accelerated compared to the bulk, i.e. the glass transition temperature increases with h !

The enhancement of the mobility in thin films originates from the surfaces, and this effect is larger at the free than at the supported surface. Thus, the films have lower Tc and Tg values relative to the bulk. As can be seen from the figure on the right, the film thickness dependence of our MD results can be well parametrized by

Tg(h) = Tg / (1+h0 / h),

(and similar for Tc) a function proposed in recent experiments on supported polystyrene (PS) films. The PS results are also shown as well as results from Monte Carlo (MC) simulations of a chemically realistic model for polypropylene (PP).


Related publications

  1. F. Varnik, J. Baschnagel, K. Binder
    Confinement effects on the slow dynamics of a supercooled polymer melt:
    Rouse modes and the incoherent scattering function

    Eur. Phys. J. E 12, 167 (2003).

  2. H. Meyer, J. Baschnagel
    Structure Formation of Supercooled Polymers in Confined Geometries:
    A Molecular Dynamics Simulation Study

    Eur. Phys. J. E 12, 147 (2003).

  3. J. Baschnagel, F. Varnik
    Computer simulations of supercooled polymer melts in the bulk and in confined geometry
    J. Phys.: Condens. Matter 17, R851-R953 (2005).
  4. S. Peter, H. Meyer, J. Baschnagel
    Thickness-dependent Reduction of the Glass Transition Temperature in Thin Polymer Films with a Free Surface
    J. Polym. Sci. B 44, 2951 (2006).

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